From: Development and characterization of a high-solids deacetylation process
Experimental variable | Axial (−2) | −1 | Center point (0) | +1 | Axial (+2) |
---|---|---|---|---|---|
Solids loading (wt%) | 10 | 15 | 20 | 25 | 30 |
Temperature (°C) | 60 | 70 | 80 | 90 | 100a |
Time (min) | 45 | 60 | 75 | 90 | 105 |
NaOH loading (g/g acetate) | 0.5 | 1 | 1.5 | 2 | 2.5 |