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Table 2 Chemical shifts and integration regions for pyrolysis oil derivatized with TMDP in a quantitative 31 P NMR

From: The use of combination of zeolites to pursue integrated refined pyrolysis oil from kraft lignin

Functional group

Integration region (ppm)

endo-N-hydroxy-5-norbornene-2,3-dicarboximide (NHND, internal standard)

151.0 - 152.8

Aliphatic OH

150.0 - 145.5

C5 substituted guaiacyl phenolic OH

β-5

144.7 - 142.8

4-O-5

142.8 - 141.7

5-5

141.7 - 140.2

Guaiacyl phenolic OH

140.2 - 139.0

Catechol type OH

139.0 - 138.2

p-hydroxy-phenyl OH

138.2 - 137.3

Carboxylic acid-OH

136.6 - 133.6