No. | Comp 8 (kg) | MeNH2 sol. (L) | MeOH (L) | Temp (°C) | Yield (%) | Quality details by HPLC (%) | |||||
---|---|---|---|---|---|---|---|---|---|---|---|
9 | 8 | 7 | 6 | 5 | 16 | ||||||
1 | 2.88 | 2.93 | 28.8 | 60–65 | 87.5 | 99.76 | ND | 0.04 | ND | ND | ND |
2 | 2.87 | 2.92 | 28.7 | 60–65 | 86.0 | 99.80 | ND | 0.02 | ND | ND | ND |
3 | 2.90 | 2.95 | 29.0 | 60–65 | 85.0 | 99.86 | 0.01 | 0.02 | ND | ND | ND |